Saccharina japonica seaweed-derived biochar production at various pyrolysis temperatures

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Abstract

Biochars from the seaweed Saccharina japonica were obtained by stepwise pyrolysis at temperatures of 300, 400, 500, 700, 900 °C. Its characteristics and properties were studied: elemental composition, specific surface area and total pore volume, particle size distribution, as well as characteristic functional groups were determined using IR-Fourier spectroscopy. With an increase in the pyrolysis temperature from 300 °C to 900 °C, the biochar yield decreases from 50.4% to 22.7%. The biochar obtained at 500 °C has the largest specific surface area – 38.6 m2/g. As the pyrolysis temperature increases, the elemental composition of the biochar changes: the content of carbon, hydrogen, nitrogen decreases, and the content of sulfur and oxygen increases.

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About the authors

M. V. Tsvetkov

Federal Research Center for Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences

Author for correspondence.
Email: tsvetkovmv@gmail.com
Russian Federation, Chernogolovka

A. Yu. Zaichenko

Federal Research Center for Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences

Email: tsvetkovmv@gmail.com
Russian Federation, Chernogolovka

D. N. Podlesniy

Federal Research Center for Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences

Email: tsvetkovmv@gmail.com
Russian Federation, Chernogolovka

A. A. Glukhov

Federal Research Center for Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences

Email: tsvetkovmv@gmail.com
Russian Federation, Chernogolovka

Yu. Yu. Tsvetkova

Federal Research Center for Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences

Email: tsvetkovmv@gmail.com
Russian Federation, Chernogolovka

M. A. Repina

Sakhalin State University

Email: tsvetkovmv@gmail.com
Russian Federation, Yuzhno-Sakhalinsk

E. A. Salgansky

Federal Research Center for Problems of Chemical Physics and Medicinal Chemistry, Russian Academy of Sciences

Email: tsvetkovmv@gmail.com
Russian Federation, Chernogolovka

E. M. Latkovskaya

Sakhalin State University

Email: tsvetkovmv@gmail.com
Russian Federation, Yuzhno-Sakhalinsk

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Supplementary files

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2. Fig. 1. Experimental setup diagram: 1 – nitrogen cylinder, 2 – flow regulator, 3 – electric coil, 4 – muffle furnace, 5 – sample, 6 – thermocouple, 7 – quartz reactor, 8 – water seal

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3. Fig. 2. Photographs of biochars SJ300 (left) and SJ400 (right)

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4. Fig. 3. Micrograph and energy dispersive X-ray (EDX) spectrum of SJ700 biochar

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5. Fig. 4. Fourier transform IR spectra of biochars obtained from the alga Saccharina japonica by pyrolysis at different temperatures

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